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  • 1.  ASTM Grain Size - Sizes Less than 1

    Posted 06-30-2023 10:49

    Hello!

    Another ASTM question for you all.  I recently gave a presentation on grain size measurement and, as usual, I was humbled by how much I did not understand before going into writing the slideshow.

    One facet that I have been unable to grasp is how ASTM Grain Sizes of less than 1 are defined.  Comparison charts exist, and E112 describes, grain sizes of 0.5, 0 and 00.  However, the mathematical definition of ASTM Grain size (NAE=2G-1) would give non-sensical values of grain density if you plugged in 0.5 or 0 in for G.  00 is not even a proper number.

    If I had to guess, I think the sizes are divisions of G = 1 (1 grain/in2 at 100X) into quarters.  The grain density for G = 0.5, 0, and 00 are 0.71, 0.5, and 0.25 grains/in2 at 100X respectively.  I think there is a simple division of the grain density going on, with a then somewhat arbitrary assignment of a grain number to represent it. 

    Anyone know if I'm on the right track there, or maybe have some better knowledge to what the reasoning is?  The mathematical description just seems to break down at this point.

    Thanks,

    Stephen



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    Stephen Rooney
    R&D Metallurgist
    Ellwood Materials Technologies
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    IMAT Conference & Expo


  • 2.  RE: ASTM Grain Size - Sizes Less than 1

    Posted 07-01-2023 14:57
    The formula does work. 0 = 0, 00 = -1, etc.
    For very fine or coarse grain sizes, it may be necessary to change magnification.
    Doubling the magnification adds 2 to the apparent grain size.
    Halving the magnification subtracts 2 from the apparent grain size. 

    --
    John Grubb



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  • 3.  RE: ASTM Grain Size - Sizes Less than 1

    Posted 07-01-2023 21:32

    The only designation that doesn't make sense to me is the "00".  The formula works for all of the "real" grain size values, just not the "00"... which is apparently ASTM's secret code for "-1".



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    David Coulston
    Niles MI
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  • 4.  RE: ASTM Grain Size - Sizes Less than 1

    Posted 07-02-2023 10:51

    Stephen:

    Math aside, what actual applications involve grain sizes of the order of 1 sq. inch?  In my professional life I was dealing with grain sizes of about 8 to 12 ASTM grain size numbers.



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    Nassos Lazaridis
    Owner
    NAL Consulting, retired
    Granger IN
    (574) 273-1979
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  • 5.  RE: ASTM Grain Size - Sizes Less than 1

    Posted 07-02-2023 12:39
    Grain sizes on the order of 1 inch diameter are seen in ingots and other large castings. Anisotropic flow leads to slip incompatibility and greatly reduced ductility. 

    --
    John Grubb



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  • 6.  RE: ASTM Grain Size - Sizes Less than 1

    Posted 07-03-2023 10:02

    I've seen these large grain sizes on turbine blades, where the ultimate goal is to make a single-grain directionally solidified component.



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    Aaron Tanzer
    Principal Research Engineer
    University of Dayton Research Institute
    Beavercreek OH
    (407) 247-9557
    ------------------------------

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  • 7.  RE: ASTM Grain Size - Sizes Less than 1

    Posted 07-03-2023 13:37
    Stephen and co -

    There is nothing wrong with that formula or Table 4.
    See below.

    image.png

    However, for large grains, you really should be using Table 3, for macroscopic
    grain size.

    More importantly, you can refer specific questions about E112 to its subcommittee.
    See below.   Travis can put you in contact with the correct person, likely George VdV.

    regards,
    - Jim


    Committee E04 Officers and Staff Support
    Staff Manager: Travis Murdock (tmurdock@astm.org)

    Committee Officers
    Editor: Emilie Whealen
    Chair: Gabriel Lucas
    Member-At-Large: George F. Vander Voort
    Second Vice-Chair: Janet Gbur
    Administrative Assistant: Jill Dicicco
    Member-At-Large: John G. Chir
    Recording Secretary: Lesley D. Frame
    First Vice-Chair: Margaret P. Willis
    Membership Secretary: Matt Simons
    Staff Manager: Travis Murdock




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  • 8.  RE: ASTM Grain Size - Sizes Less than 1

    Posted 07-06-2023 12:27

    Thanks all.  I made a math error; the formula does work fine.  Good to be reminded of the macroscope table as well.  I also was unaware that 0 and 00 were "code" for negative numbers.

    Nassos - I've run into large grains such as this in large open die forgings where local explosive grain growth or recrystallization can occur.  I typically report grain sizes like these in grain diameter terms (X μm at 1X, etc.) but some colleagues are more comfortable with ASTM G grain sizes.

    Thanks!

    Stephen



    ------------------------------
    Stephen Rooney
    R&D Metallurgist
    Ellwood Materials Technologies
    ------------------------------

    IMAT Conference & Expo