What tools do you have available? If you have a metallography lab, specific defects can be marked (typically with scribe lines) mounted in clear epoxy and cross sectioned. Depending on the skill of the metallographer, sub millimeter defects can be successfully cross sectioned. Optical examination can distinguish some of the different layers, but SEM/EDS is really needed to identify the elements present in the defect. There are methods to examine the different surfaces. This typically involves stripping the paint with a heated phenol based solution or other paint stripping solution. Unfortunately this will remove all paint layers and not specific ones. The pretreatment could then be examined in a SEM/EDS system. After examining the pretreatment, the pretreatment could then be stripped with the appropriate solution (depends on pretreatment) and then the substrate surface can be examined.
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Paul Janavicius
Lead Research Engineer
Cleveland-Cliffs Steel Corporation
Middletown OH
(513) 425-2670
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