Hi John
It would be helpful to know the roughness and transparency of these films as ellipsometry is a very useful technique with low absorbance and low scattering films.
Regarding X-ray diffraction, the application of peak broadening using the Scherer equation is only valid up to crystallite sizes of about 100 nm, and then only after instrumental peak broadening has been quantified and removed.
I look forward to hearing what you find to be useful here.
Harold
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Harold Ackler
Clinical Associate Professor
Micron School of Materials Science and Engineering
Boise State University, Boise ID
408-230-7277 cell
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Original Message:
Sent: 02-16-2026 18:29
From: John Merrill
Subject: Non-destructive CVD thickness measurement
When using CVD to deposit polycrystalline diamond onto a silicon carbide base, there are instances where one must measure the deposition layer (say about 10 micron) without cross-sectioning the finished product or applying the same coating to a sample that can be destructively measured. There must be a way aerospace or automotive suppliers do this, possibly with x-ray absorbance or wavelength bounceback.
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John Merrill
Principal Engineer
EagleBurgmann | Freudenberg
Matthews NC
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